#1 - 0.5 uL 0.5 mg/mL standards #2 - 0.5 uL 1/11 of 16.5 mg/mL red oil 0.2 mg/mL phenanthrane in methanol #3 - 0.5 uL 1/11 of 16.8 mg/mL red oil 0.2 mg/mL phenanthrane in dodecane #4 - 0.5 uL dodecane #5 - 0.5 uL 1/11 of 16.8 mg/mL red oil 0.2 mg/mL phenanthrane in dodecane 30 uL MSTFA added to 300 uL 1/11 dodecane solution incubated 90 deg C x 20 min #6- 0.5 uL injected